Table 1 Structure determination statistics.
Native | EMTS | K2PtCl4 | |
|---|---|---|---|
Resolution (Å) | 2.80 | 2.8 | 3.0 |
Space group | R32 | R32 | R32 |
Unit-cell dimensions (Å) | a = b = 181.14 c = 240.13 | a = b = 179.76 c = 240.90 | a = b = 181.27 c = 240.02 |
Completeness (%) | 100 (100) | 99.9 (100) | 95.8 (69.6) |
Redundancy | 10.9 | 10.2 | 5.1 |
Rsym (%) | 9.8 (59.4) | 8.4 (60.9) | 11.5 (38.3) |
R merge (%) | - | 24.2 | 18.3 |
Heavy atom sites | - | 20 | 13 |
Isomorphous phasing power | - | 1.25/1.22 | 1.28/1.36 |
Anomalous phasing power | - | 0.482 | 0.335 |
Isomorphous R cullis | - | 0.784/0.722 | 0.717/0.595 |
Anomalous R cullis | - | 0.656 | 0.947 |
Overall FOM | 0.344/0.426 | ||
Resolution (Å) | 50.0-2.79 | ||
R f (%) | 21.8 | ||
R free (%) | 24.1 | ||
Protein atoms | 3529 | ||
Water molecules | 93 |