Space group | P21 |
---|---|
Unit cell dimensions | |
a (Å) | 42.2 |
b (Å) | 64.3 |
c (Å) | 48.6 |
β (°) | 102.1 |
Number of molecules in the unit cell | 2 |
Resolution range (Å) | 36.0 - 1.2 |
The range of the highest shell | 1.24 - 1.20 |
Total number of measured reflections | 727277 |
Number of unique reflections | 62459 |
Rsym (%) | 5.0(22.1) |
I/σ(I) | 17.8(3.6) |
Completeness of data (%) | 98.5(87.1) |
Rcryst (%) | 15.8 |
Rfree (%) 5% of reflections | 18.6 |
Protein atoms | 2101 |
Water oxygen atoms | 434 |
Phosphate ion atoms (1) | 5 |
Atoms from PEG | 40 |
R.m.s.d in bond lengths (Å) | 0.008 |
R.m.s.d in bond angles (°) | 1.2 |
R.m.s.d in torsion angles (°) | 16.8 |
B-factors (Å 2 ) | |
B-factor from Wilson plot (Å2) | 12.3 |
Mean B-factor for main chain atoms (Å2) | 11.2 |
Mean B-factor for side chain and water atoms (Å2) | 19.2 |
Mean B-factor for all atoms(Å2) | 15.8 |
Ramachandran's ϕ, ψ map | |
Residues in the most favoured regions (%) | 90.4 |
Residues in the additionally allowed regions (%) | 9.3 |
Residues in the generously allowed regions (%) | 0.3 |
PDB ID | 3MU7 |