| CPH/IP5(6) |
---|---|
Date Collection | Â |
   Space group | C2 |
   Unit-cell parameters (Å) | a = 82.5, b = 47.6 and c = 87.6 α = β = γ = 90 |
   No. of molecules in asymmetric unit | 3 |
   Resolution range (Å)a | 50.00 - 1.65 (1.71-1.65) |
   Unique reflections | 39 679 |
   Data Redundancya | 3.5 (2.5) |
   Completeness (%)a | 98.47 (91.4) |
   I/σ(I)a | 26.6 (2.4) |
   R merge (%)a | 3.9 (36.3) |
Model and refinement | Â |
   Resolution range (Å)a | 87.71-1.75 (1.79-1.75) |
   R work (%) | 18.0 |
   R free (%) | 24.3 |
   No. of reflections | 31 402 (28 793 in working set and 2609 in test set) |
   No. of waters | 315 |
   r.m.s.d bond lengths (Å) | 0.024 |
   r.m.s.d bond angles (°) | 2.3 |
   Average B factor (Å2) | 40.1 |
   PDB code | 2I5C |