hDNPEP·Zn2+·ABH | |
---|---|
PDB accession code | 4DYO |
Data collection | |
Beamline | Diamond Light Source, I03 |
Wavelength (Å) | 0.9763 |
Spacegroup | F 432 |
Resolution rangea (Å) | 56.11 – 2.20 (2.32 – 2.20) |
Unit cell dimensions | a = b = c = 224.60 Å; α = β = γ = 90.0° |
No. unique reflectionsa | 32,192 (4,486) |
Completenessa (%) | 99.6 (97.5) |
I/σIa | 10.4 (2.2) |
Rmergea (%); Rpima (%) | 17.9 (83.3); 5.5 (29.7) |
Redundancya | 10.8 (8.0) |
Wilson B factor (Å2) | 28.5 |
Refinement | |
No. atoms in refinement (P/L/M/O)c | 3585/10/2/358 |
Rfact (%) | 15.5 |
Rfree (%) | 19.5 |
Bf (P/L/M/O)c (Å2) | 26/30/28/28 |
rms deviation bond lengthb (Å) | 0.015 |
rms deviation bond angleb (°) | 1.5 |
Molprobity | |
Ramachandran favoured | 97.1 |
Ramachandran allowed | 99.8 |