|
Data collection
| |
|---|
|
Space group
|
P41
|
|
unit cell (Å)
|
a=b=80.1 c=125.8
|
|
Resolution (Å)
|
50–2.15
|
|
Completeness
|
95.5 (95.9)a
|
|
Redundancy
|
10.0 (7.8)
|
|
I/σ(I)
|
24.5 (7.2)
|
|
Rsym (%)b
|
10.4 (47.4)
|
|
Refinement
| |
|
Resolution
|
50-2.0
|
|
Rwork/Rfree (%)c
|
19.73/23. 51
|
|
RMSD
| |
|
Bond lengths (Å)
|
0.007
|
|
Bond angles (°)
|
1.070
|
|
Ramachandran plot (%)d
| |
|
Most favored (%)
|
92.9
|
|
Additionally allowed (%)
|
6.9
|
|
Generously allowed (%)
|
0.2
|
|
Disallowed (%)
|
0.0
|
- a Values in parentheses are for reflections in the highest resolution shell.
- bRsym=∑
hkl
∑
i
|I(hkl)
i
-<I(hkl)>|/∑
hkl
∑I<I(hkl)
i
>over i observations.
- c Value of Rfree for 3.91% of randomly selected reflections excluded from refinement.
- d As defined in PROCHECK.
