Data collection statistics
a
| | |
Beamline
|
SPring8 BL44XU
|
SPring8 BL44XU
|
Wavelength (Å)
|
0.9000
|
0.9790
|
Oscillation range (º)
|
180
|
1080
|
Space group
|
C 2
|
C 2
|
Cell parameters (Å)
|
a = 180.2, b = 52.9, c = 78.4
|
a = 181.6, b = 53.5, c = 79.0
|
Resolution range (Å)
|
50.0 – 1.90 (1.94 – 1.90)
|
50.0 – 2.30 (2.34 – 2.30)
|
Observed reflections
|
215,719
|
702,336
|
Unique reflections
|
58,464
|
32,931
|
Completeness (%)
|
99.5 (99.3)
|
99.8 (99.2)
|
R
merge(I)b
|
0.071 (0.586)
|
0.175 (> 1)
|
I / σ(I)
|
25.0 (2.5)
|
16.3 (3.6)
|
Refinement statistics
| | |
Resolution range (Å)
|
50.0 – 1.90
| |
No. of protein atoms
|
5,644
| |
No. of water molecules
|
553
| |
R
work
/R
free
c
|
0.164/0.202 (0.244/0.304)
| |
Rmsdd from ideality bond length (Å)
|
0.007
| |
angles (º)
|
1.1
| |
Ramachandran plot (%)e
| | |
Favored region
|
98.3
| |
Allowed region
|
1.7
| |
Outlier region
|
0.0
| |