Data collection | |
---|---|
X-ray source | Diamond I03 |
Wavelength (Å) | 0.97630 |
Space group | P 21212 |
Unit cell (Å) | a = 140.4, b = 174.2, c = 81.7 |
Resolution range (Å) | 30.0 – 2.50 (2.59-2.50) |
Unique reflections | 71197 (7000) |
Completeness (%) | 100 (100) |
Redundancy | 12.3 (10.5) |
Average I/σI | 14.9 (2.1) |
Rmerge | 0.157 (−−) |
Refinement | |
Resolution range (Å) | 30.0 – 2.50 |
No. of atoms (protein/other atoms) | 11212/323 |
Rms bond length deviation (Å) | 0.008 |
Rms bond angle deviation (°) | 1.2 |
Mean B-factor (protein/other atoms[Å2]) | 38/54 |
Residues in preferred regions (%) | 1112 (89.5) |
Residues in allowed regions (%) | 128 (10.3) |
Residues in disallowed regions (%) | 3 (0.2) |