Table 1 Statistics for crystallographic structure determination

Data collection site

In house

Detector

MAR345

Wavelength (Å)

1.5418

Resolution range (Å)

30.0-3.1 (3.21-3.10)

Number of unique reflections

13636

Redundancy

3.8 (2.8)

Completeness (%)

94.8 (87.9)

Average I/σ(I)

8.5 (2.3)

Rmerge^a

0.149 (0.494)

Resolution range (Å)

30.0-3.1 (3.18-3.1)

R-factor†(R_work/R_free)^b

25.7/28.9

Number of protein atoms

5206

Average B factor (Ų)

42.3

Rms bond length deviation (Å)

0.012

Rms bond angle deviation (°)

1.42