| SAD | Native |
---|---|---|
Data collection | Â | Â |
   Resolution (Å) | 30–2.3 | 50–2.1 |
   Wavelength (Å) | 0.9792 | 0.9795 |
   Total reflections | 1,996,840 | 1,197,490 |
   Unique reflections | 29,848 | 38,527 |
   Completeness (%) | 99.8 (99.8)a | 99.9 (100)a |
   Rsym (%)b | 11.9 (32.2) | 13.7 (64.3) |
   Average I/σ(I) | 30.4 (6.7) | 17.0 (3.1) |
Refinement | Â | Â |
   Resolution (Å) | 50–2.1 |  |
   Rcryst (%)c | 22.3 |  |
   Rfree (%)d | 26.4 |  |
   Protein atoms | 4,469 |  |
   Water molecules | 138 |  |
   RMS deviations |  |  |
Bond lengths (Ã…) | 0.0095 | Â |
Bond angles (°) | 1.50 |  |
   Ramachandran plot (%)e |  |  |
Most favored | 92.0 | Â |
Additionally allowed | 7.2 | Â |
Generally allowed | 0.8 | Â |
Disallowed | 0 | Â |