Beamline | ID14-2 (ESRF, Grenoble) |
---|---|
Wavelength (Å) | 0.933 |
Space group | C 2221 |
Unit cell parameters | |
a, b, c (Å) | 101.5, 185.4, 106.9 |
Resolution range (Å) | 20–2.60 (2.69–2.60)a |
Unique reflections | 30931 (3028) |
Completeness (%) | 98.7 (97.4) |
< I/σ(I) > | 24.5 (2.5) |
Multiplicity | 4.9 (3.8) |
Rsymb (%) | 6.8 (25.8) |
Rcryst/Rfreec (%) | 22.3/24.5 |
No. of non-hydrogen atoms | 5466 |
Protein | 5342 |
Solvent | 124 |
Average B-factors (Å2) | 78 |
Main chain – subunit A/B/C | 68/89/72 |
Side-chain – subunit A/B/C | 71/91/76 |
Solvent | 81 |
Wilson B-factor | 77.1 |
RMSD bonds (Å) | 0.011 |
RMSD angles (°) | 1.26 |
Ramachandran statisticsd | |
Core | 91.4% |
Allowed | 7.9% |
Generous | 0.7% |
Disallowed | None |