Grb7 SH2 | Â |
---|---|
Data Collection | Â |
Space group | P2 1 2 1 2 1 |
Unit Cell (Ã…) | a = 62.6 |
 | b = 63.9 |
 | c = 105.7 |
 | α = β = γ = 90° |
Molecules in the ASU | 4 |
Resolution range (Å)a | 44 – 2.1 (2.18 – 2.1) |
Observations | 79384 |
Unique reflections | 25401 |
Completeness (%)a | 99.1 (99.4) |
I/σa | 12.6 (2.2) |
Rmerge (%)a, b | 8.4 (50.5) |
Wilson B (Ã…)a | 28.4 |
Refinement | Â |
Resolution limits (Å)a | 30 – 2.10 (2.15 – 2.10) |
No. of reflectionsa | 23949 (1731) |
Rcryst (%)a | 20.1 (25.4) |
Rfree (%)a, c | 25.5 (28.9) |
Protein atoms | 3733 |
Water molecules | 181 |
Other molecules | 7 SO42- |
r.m.s.d. from ideal values ideaiations | Â |
Bond lengths (Ã…) | 0.014 |
Bond angles (°) | 1.486 |
Average B-factors (Ã…)3 | Â |
Protein | 38.1 |
Water | 40.6 |
Ions | 58.7 |