Structure | M. smegmatis IspF |
---|---|
Unit cell, a, b, c (Ã…) | 159.1, 159.1, 54.2 |
Resolution range (Ã…) | 51.3-2.2 Ã… |
No. of observations | 117,125 |
No. of unique reflections | 33,193 |
Completeness (%) | 95.4 (76.3)†|
<I/σ(I)> | 6.0(1.7) |
Rsym (%) | 8.1(34.6) |
Multiplicity | 3.5(2.1) |
Wilson B (Å2)/DPI (Å)‡ | 28.1/0.16 |
Protein residues | 461 |
Water molecules | 272 |
CDP/Zn2+ molecules (occupancy) | 3(1)/3(0.75/0.5/0.75) |
IPP molecules (occupancy) | 1(0.5) |
PEG/Glycerol/Ethylene glycol/Acetate molecules | 2/3/2/1 |
Rwork/Rfree (%) | 16.3/20.6 |
Average B (Ã…2) | Â |
   Subunit A/B/C overall | 30.7/19.7/31.8 |
   All main/side chain | 25.9/29.3 |
   Waters | 35.8 |
   CDP/Zn2+ | 25.0/36.0 |
   IPP | 47.5 |
   PEG/Glycerol/Ethylene glycol/Acetate | 45.3/58.4/28.5/38.9 |
RMS bond lengths (Ã…) | 0.013 |
RMS bond angles (°) | 1.570 |
PDB Code | 2UZH |