D86A | D247A | E342A | E342A/Raffinose | |
---|---|---|---|---|
Space group | P 212121 | P 212121 | P 212121, 1 | P 212121 |
Unit cell | ||||
a (Å) | 51.1 | 51.2 | 51.1 | 52.2 |
b (Å) | 67.1 | 67.4 | 67.3 | 66.7 |
c (Å) | 123.7 | 123.8 | 123.6 | 124.0 |
Wavelength (Å) | 1.5418 | 1.5418 | 1.5418 | 1.5418 |
Resolution range (Å) | 30-2.07 | 30-2.07 | 30-2.07 | 30-2.03 |
Observations (I/σ(I) > 0) | 80868 | 232052 | 118645 | 139045 |
Unique reflections (I/σ(I) > 0) | 24114 | 26627 | 26368 | 27688 |
Last shell (Å) | 2.14-2.07 | 2.14-2.07 | 2.14-2.07 | 2.10-2.03 |
Rsym (%)a,b | 3.9 (6.4) | 3.8 (6.8) | 3.7 (6.8) | 5.3 (9.7) |
<I/σ(I)> | 24.7 (25.0) | 25.0 (25.1) | 25.0 (25.1) | 25.1 (25.5) |
Completeness (%) | 90.8 (88.1) | 99.5 (99.0) | 98.8 (98.8) | 98.2 (98.1) |
Redundancy | 3.4 (3.3) | 8.7 (8.1) | 4.5 (4.3) | 5.0 (4.5) |