From: Interactions between the quality control ubiquitin ligase CHIP and ubiquitin conjugating enzymes
 | CHIP U-box: UbcH5a complex |
---|---|
Data Collection | Â |
Space group | P212121 |
Unit cell | Â |
   a, b, c (Å) | 79.0, 93.4, 144.0 |
   α,β,γ (°) | 90, 90, 90 |
No. molecules/asymmetric unit | 2 CHIP, 2 UbcH5a |
Resolution (Ã…) | 55.00-2.90 (3.00-2.90)a |
Unique reflections | 24283 |
Completeness (%) | 99.9 (100) |
Redundancy | 3.40 (3.42) |
I/σ | 8.5 (1.6) |
Rmerge(%)b | 8.0 (46.6) |
Refinement | Â |
Resolution (Ã…) | 53.2-2.90 (3.08-2.90) |
Rwork(%)c | 24.0 |
Rfree(%)d | 27.2 |
Protein atoms | 3518 |
Waters | 4 |
Other atoms | 3 |
Average B factor (Ã…2) | 65.0 |
r.m.s.d. – bond lengths (Å) | 0.007 |
r.m.s.d. – bond angles (°) | 1.4 |
r.m.s.d. – dihedrals (°) | 23.4 |
r.m.s.d. – improper angles (°) | 1.1 |
Ramachandran plot (%) | Â |
   Most favored and allowed | 97.6 |
   Generously Allowed | 2.4 |
   Disallowed | 0.0 |
PDB ID code | 2 OXQ |