Table 1 Data collection and refinement statistics

Space Group

P2₁

P2₁2₁2₁

Unit Cell (Å)

a = 56.93

a = 95.60

b = 107.16

b = 210.77

c = 99.76

c = 228.08

β = 100.68

Resolution (Å)

2.01

2.9

Unique Reflections

72707

102839

Multiplicity (Last shell)

2.7 (2.5)

11.7 (10.4)

Completeness (Last shell)

96.3 (92.7)

100 (99.9)

R_pim

0.09

0.116

 R_work

18.0

18.3

 R_free

21.6

22.0

 Rms Bond/angle

0.01/1.7

0.01/1.1