Table 2 Data processing and structure refinement statistics for P2-F57A
Space group | P43212 | C2 [26] | P212121 |
|---|---|---|---|
Unit cell dimensions | a = b = 58.61 Å, c = 76.96 Å α = β = γ = 90° | a = 112.76 Å, b = 36.08 Å, c = 31.17 Å, α = γ = 90°, β = 96.87° | a = 52.12 Å, b = 76.11 Å, c = 138.43 Å, α = β = γ = 90° |
Wavelength (Å) | 1.10 | 1.10 | 1.10 |
Resolution range (Å) | 20–1.59 (1.63–1.59) | 20–1.27 (1.30–1.27) | 20–1.95 (2.00–1.95) |
<I/σ(I)> | 19.1 (1.0) | 8.2 (1.2) | 11.6 (2.3) |
Rsym (%) | 6.5 (111.4) | 7.6 (60.7) | 15.8 (75.0) |
Rmeas (%) | 7.2 (129.6) | 9.2 (78.1) | 17.3 (82.1) |
Completeness (%) | 98.7 (92.7) | 96.8 (77.4) | 99.1 (98.7) |
Redundancy | 5.7 (3.2) | 2.9 (1.8) | 6.0 (6.0) |
CC1/2 (%) | 99.9 (39.9) | 99.6 (43.6) | 99.4 (75.4) |
Wilson B factor (Å2) | 27.2 | 16.9 | 20.2 |
Rcryst (%) | 18.6 | 17.1 | 18.8 |
Rfree (%) | 21.6 | 22.4 | 23.6 |
rmsd bond lengths (Å) | 0.012 | 0.009 | 0.005 |
rmsd bond angles (°) | 1.3 | 1.2 | 0.9 |
Ramachandran favoured/allowed (%) | 100/100 | 99.3/100 | 98.1/100 |
# molecules in asymmetric unit | 1 | 1 | 4 |
MolProbity score (percentile) | 1.25 (97th) | 1.48 (79th) | 1.32 (99th) |
PDB entry | 6EW2 | 6EW4 | 6EW5 |