Data collection | |
X-ray source | ESRF ID29 |
Space group | P3221 |
Unit cell (Å) | a = b = 84.41, c = 198.74 |
Resolution (Å) | 30 – 2.00 (2.05 – 2.00) |
Wavelength (Å) | 0.9724 |
No. unique reflections | 55 287 |
Multiplicity | 3.3 (3.3) |
Completeness (%) | 98.0 (98.2) |
Mean (<I> /<σI>) | 17.4 (2.6) |
R-sym (%)a | 4.5 (52.8) |
Wilson B-factor (Å2) | 40.2 |
Refinement | |
PDB entry | 4TRT |
R-factor (all reflections) (%) | 20.0 |
R-free (%)b | 23.5 |
Number of atoms | 5758 |
Number of water molecules | 292 |
RMSD bond lengths (Å) | 0.008 |
RMSD bond angles (°) | 1.255 |
Average B-factor (Å2) | |
All atoms | 46.4 |
Protein | 46.2 |
Water | 49.2 |
Ramachandran plot | |
Favoured regions (%) | 713 (97.7) |
Allowed regions (%) | 17 (2.3) |
Outliers (%) | 0 (0) |