Table 1 Crystallographic Data and Refinement Statistics

Beamline

ALS 8.2.2

Wavelength (Å)

1.00

Space group

P2₁2₁2₁

Cell (Å)

83.9 93.7 136.9

Resolution (Å)

50.00-3.00 (3.11-3.00)

R_sym (%)

14.8 (57.4)

I/σ

10.7 (1.9)

Completeness (%)

97.9 (88.2)

Redundancy

5.2 (4.0)

Refinement

Reflections

22002

   Test set

1121

Number of atoms

6761

   Protein

6354

   Nucleic acid

407

R_factor (%)

22.3

R_free (%)

28.0

r.m.s. deviation, bond lengths (Å)

.003

r.m.s. deviation, bond angles (°)

.667