Table 1 Crystallographic and Data Refinement Statistics
| Â | C-PH/Ins(1,2,3,5,6)P5 |
|---|---|
Date Collection | Â |
   Space group | P212121 |
   Unit-cell parameters (Å) | a = 32.2, b = 47.7 and c = 64.1 α = β = γ = 90 |
   No. of molecules in asymmetric unit | 1 |
   Resolution range (Å)a | 32.03 – 1.35 (1.40–1.35) |
   Unique reflections | 21 808 |
   Data Redundancya | 12.21 (7.17) |
   Completeness (%)a | 97.7 (95.9) |
   I/σ(I)a | 25.1 (3.9) |
   R merge (%)a | 4.4 (45.4) |
Model and refinement | Â |
   Resolution range (Å)a | 38.26 – 1.35 (1.39–1.35) |
   R work (%) | 18.0 |
   R free (%) | 20.8 |
   No. of reflections | 20 722 (19 638 in working set and 1084 in test set) |
   Cutoff criterion |  |
   No. of amino acid residues/atoms | 99/999 |
   No. of waters | 125 |
   r.m.s.d bond lengths (Å) | 0.034 |
   r.m.s.d bond angles (°) | 3.2 |
   Average B factor (Å2) | 23.2 |
   PDB code | 2I5F |