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Table 2 Data collection and refinement statistics

From: New insights into the molecular mechanism of the Rab GTPase Sec4p activation

  Sec4pV29 Sec4pV29.Sec2p complex
Data collection statistics
Space group P21 I222
Unit cell   116.900 119.280 122.860
a, b, c (Å) 31.720, 75.450, 66.230  
β (°) 91.58  
Wavelength (Å) 1.54180 1.08090
Resolution range (Å) 28.30–1.90 (2.00-1.90) 60.00–2.90 (2.90–3.06)
No. reflections/no. unique reflections 39912/23244 152363/19373
Redundancy 1.7 (1.6) 7.9 (8.1)
Completeness (%) 94.8 (98.3) 99.8 (100)
Rmeas (%) 7.1 (38.9) 9.0 (54.5)
I/σ (I) 9.1 (2.3) 5.1 (1.5)
  Refinement statistics
Resolution range (Å) 28.30–1.90 59.64–2.90
no. of reflections (working data/test data) 21713/1170 17371/879
R-factor/R-free (%) 23.9/29.7 25.8/29.5
Protein atoms 2598 2867
Water molecules 464 16
Mean B value/Wilson B value (protein, all atoms) (Å2) 17.2/22.0 51.5/66.8
Mean B value (ligand) (Å2) 16.3 74.2
rmsd bond length (Å) 0.011 0.012
rmsd bond angle (°) 1.432 1.613